AbstractAbout AuthorsReferences
The results of studies of IR transmission spectra of carbon nanomaterials (CNM) obtained by gas pyrolysis and subjected to heating in the presence of water vapor are presented. The method of infrared spectroscopy makes it possible to study the composition and structure of various substances. At this, a very small amount of material is sufficient for conducting research, and the material itself does not require special preliminary preparation. For many systems, the method of infrared spectroscopy makes it possible to obtain information about the structure of the surface, characterize the centers of adsorption and their interaction with the adsorbed substance. The purpose of the study was to determine the effect of high-temperature steam-gas treatment on the change in the phase composition of the CNM. The obtained data explain the previously assumed mechanism of increasing the strength set of cement stone.
S.A. ZHDANOK1, Doctor of Sciences (Physics and Mathematics);
E.N. POLONINA2, Engineer,
S.N. LEONOVICH2, Doctor of Sciences (Engineering), Foreign Member of RAACS (Russian Academy of Architecture and Construction Sciences)
E.N. POLONINA2, Engineer,
S.N. LEONOVICH2, Doctor of Sciences (Engineering), Foreign Member of RAACS (Russian Academy of Architecture and Construction Sciences)
1 OOO “Advanced Research and Technologies” (room 16, 1, Sovkhoznaya Street, Leskovka, Minsk District, 223058, Republic of Belarus)
2 Belarusian National Technical University (Belarus, 220013, Minsk, Nezavisimosty Avenue, 65)
1. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrusta-lev B.M., Koleda E.A. Strength enhancement of concrete with a plasticizer on the basis of nano-structured carbon. Stroitel’nye Materialy [Construction Materials]. 2018. No. 6, pp. 67–72. DOI: https://doi.org/10.31659/0585-430X-2018-760-6-67-72 (In Russian).
2. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrustalev B.M., Koleda E.A. The effect of plasticizing additives containing carbon nanomaterial on the properties of self-compacting concrete. Vestnik grazhdanskikh inzhenerov. 2018. No. 6 (71), pp. 76–85. (In Russian).
3. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrustalev B.M., Koleda E.A. Physico-mechanical characteristics of concrete modified with a plasticizing additive based on nanostructured carbon. Inzhenerno-fizicheskii zhurnal. 2019. Vol. 92. No. 1, pp. 14–20. (In Russian).
4. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrustalev B.M., Koleda E.A. The influence of plasticizing additives based on nanostructured carbon in a self-compacting concrete mixture on its technological properties. Inzhenerno-fizicheskii zhurnal. 2019. Vol. 92. No. 2, pp. 391–396. (In Russian).
5. Smit A. Prikladnaya IK-spektroskopiya [Applied IR-Spectroscopy]. Moscow: Mir. 1982. 328 p.
6. Mikhailova E.S., Ismagilov Z.R., Kuznetsov V.V., Podyacheva O.Yu., Chichkan’ A.S., Sal’nikov A.V., Chesnokov V.V. Installation for the preparation and conduct of IR spectroscopic studies of carbon nanomaterials. Vestnik KuzGTU. 2017. No. 4 (122), pp. 155–163. (In Russian).
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9. Zinyuk R.Yu., Balykov A.G., Gavrilenko I.B., Shevyakov A.M. IK-spektroskopiya v neorganicheskoi tekhnologii [IR spectroscopy in inorganic technology]. Leningrad: Khimiya. 1983. 158 p.
10. Ovchinnikov M.M., Lavrienko M.V., Podgornyi G.N., Pakhomov P.M. The study of allotropic forms of carbon by IR spectroscopy. Fiziko-khimiya polimerov: sintez, svoistva i primenenie. 2003. No. 9, pp. 44–49. (In Russian).
11. Zhdanok S.A. [i dr.] Nanotechnology in building materials science: reality and prospects. Vestnik BNTU. 2009. No. 3, pp. 5–22. (In Russian).
12. Patent 2839 Republic of Belarus, IPC B82B 3/00. Zhdanok S.A., Krauklis A.V., Samtsov P.P., Volzhankin V.M. Installation for producing carbon nanomaterials. Publ. 06/30/2006 (In Russian).
13. Patent 15341 Republic of Belarus, IPC7 C 01B 31/02, B 82B 3/00. Zhilinsky V.V., Drozdovich V.B., Zhdanok S.A., Zharsky I.M. A method of producing carbon nanoscale materials. Publ. 08/22/2012. (In Russian).
2. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrustalev B.M., Koleda E.A. The effect of plasticizing additives containing carbon nanomaterial on the properties of self-compacting concrete. Vestnik grazhdanskikh inzhenerov. 2018. No. 6 (71), pp. 76–85. (In Russian).
3. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrustalev B.M., Koleda E.A. Physico-mechanical characteristics of concrete modified with a plasticizing additive based on nanostructured carbon. Inzhenerno-fizicheskii zhurnal. 2019. Vol. 92. No. 1, pp. 14–20. (In Russian).
4. Zhdanok S.A., Polonina E.N., Leonovich S.N., Khrustalev B.M., Koleda E.A. The influence of plasticizing additives based on nanostructured carbon in a self-compacting concrete mixture on its technological properties. Inzhenerno-fizicheskii zhurnal. 2019. Vol. 92. No. 2, pp. 391–396. (In Russian).
5. Smit A. Prikladnaya IK-spektroskopiya [Applied IR-Spectroscopy]. Moscow: Mir. 1982. 328 p.
6. Mikhailova E.S., Ismagilov Z.R., Kuznetsov V.V., Podyacheva O.Yu., Chichkan’ A.S., Sal’nikov A.V., Chesnokov V.V. Installation for the preparation and conduct of IR spectroscopic studies of carbon nanomaterials. Vestnik KuzGTU. 2017. No. 4 (122), pp. 155–163. (In Russian).
7. Kessler I. Metody infrakrasnoi spektroskopii v khimicheskom analize [Methods of infrared spectroscopy in chemical analysis]. Moscow: Mir. 1964. 288 p.
8. Iogansen A.V. Infrared structural group analysis. Khimiya i tekhnologiya topliv i masel. 1962. No. 5, pp. 16–22. (In Russian).
9. Zinyuk R.Yu., Balykov A.G., Gavrilenko I.B., Shevyakov A.M. IK-spektroskopiya v neorganicheskoi tekhnologii [IR spectroscopy in inorganic technology]. Leningrad: Khimiya. 1983. 158 p.
10. Ovchinnikov M.M., Lavrienko M.V., Podgornyi G.N., Pakhomov P.M. The study of allotropic forms of carbon by IR spectroscopy. Fiziko-khimiya polimerov: sintez, svoistva i primenenie. 2003. No. 9, pp. 44–49. (In Russian).
11. Zhdanok S.A. [i dr.] Nanotechnology in building materials science: reality and prospects. Vestnik BNTU. 2009. No. 3, pp. 5–22. (In Russian).
12. Patent 2839 Republic of Belarus, IPC B82B 3/00. Zhdanok S.A., Krauklis A.V., Samtsov P.P., Volzhankin V.M. Installation for producing carbon nanomaterials. Publ. 06/30/2006 (In Russian).
13. Patent 15341 Republic of Belarus, IPC7 C 01B 31/02, B 82B 3/00. Zhilinsky V.V., Drozdovich V.B., Zhdanok S.A., Zharsky I.M. A method of producing carbon nanoscale materials. Publ. 08/22/2012. (In Russian).
For citation: Zhdanok S.A., Polonina E.N., Leonovich S.N. IR-spectroscopy study of the degree of activation of carbon nanomaterials for modifying structural concrete. Stroitel’nye Materialy [Construction Materials]. 2020. No. 7, pp. 49–53. (In Russian). DOI: https://doi.org/10.31659/0585-430X-2020-782-7-49-53